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Transactions of the INDIAN CERAMIC SOCIETY   Vol. 36  1977
Effect of Processing Parameters on Microstructure Development and Magnetic Spectrum of Nio.3Zno.7Fez04 Ferrite: 11-Magnetic Spectrum and its Correlation with Sintering Conditions and Microstructure
S. K. GUPTA* AND A. R. DAS
Pages : 55-60
DOI : 10.1080/0371750X.1977.10840643
Abstract
Real and imaginary parts p. and p. of the initial permeability p.0 were determined on toroidal samples of Ni-Zn ferrite of nominal composition Ni0•3Zn0•7Fe20 4 using type 260-AP Boonton Q-meter in the frequency range 100 Kc/s to 10 Mc(s. Both fLo and the quality factor Q varied with the microstructure which had been well characterised in part I of this report. The product p.0Q had a maximum of 23,720 at 100 Kc/s and 2885 at 1.5 Kc/s and p.0 had maximum values of 1250 and 1572 respectively at the above frequencies for a material sintered at 1200°C for 100 hours. The Snoek relationship correlating p.0 and fr, the peak frequency of p. giving fr(fL0·1)=constant was used to relate variation of fLo with fr. The grain size also influenced the value of p.0 and the Kersten relationship p.0 = const. x D, where D is distance between domain pinning inclusions, was used to relate grain size and permeability. Sintered pellets of different stoichiometric deviations and processed by different grinding media were used for d.c. resistivity measurement. The resistivity showed a maximum value of 107 ohms-em for a 1.5 mole% Fe20 3 deficient sample ground with alumina and a minimum of 1.3 x 102 ohm-em for the material ground with steel.
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